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新工艺制备高纯钛酸铅
New method for the preparation of high purity plumbous titanate
【摘要】 通过用草酸做沉淀剂制备高纯钛酸铅的实验 ,对影响反应的多种因素进行了探索 ,并确定了合理的制备步骤及工艺条件。产品经X -射线衍射和扫描电镜分析 ,为单一PbTiO3 相 ,粒度小于 1μm ,纯度≥ 99.6 %。经应用厂家实验 ,反应良好 ,开辟了液相钛酸铅制备的一种新途径
【Abstract】 According to the experiment by using the oxalic acid as the precipitating agent to produce the high purity plumbous titanate,the factors of influencing the reaction were studied and the optimum process conditions were determined.Through the analysis of X-ray and SEM,it found that the product is a single-phase PbTiO 3 and the particle diameter is less than 1 μm and the purity of the product is more than 99.6%.This method is a new way for the preparation of liquid phase plumbous titanate.
- 【文献出处】 无机盐工业 ,Inorganic Chemicals Industry , 编辑部邮箱 ,2003年05期
- 【分类号】TQ134.11
- 【下载频次】107