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水热法合成掺杂铁离子的小管径TiO2纳米管

Preparation of Fe-doped TiO2 Nanotubes with Small Diameter by Hydrothermal Method

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【作者】 宋旭春岳林海刘波韩贵陈卫祥徐铸德

【Author】 SONG Xu Chun YUE Lin Hai LIU Bo HAN Gui CHEN Wei Xiang XU Zhu De* (Department of Chemistry, Zhejiang University, Hangzhou 310027)

【机构】 浙江大学化学系浙江大学化学系 杭州310027杭州310027杭州310027

【Abstract】 Using Fe doped titania powders as the precursor, Fe doped TiO2 nanotubes with small diameter of 10nm were obtained by hydrothermal method. The doped titania powders have two different crystalline phases, anatase and rutile of which the average particle diameters are 30.3nm and 41.7nm, receptively. The products were characterized by TEM, XRD and EDS. The results showed that Fe doped TiO2 nanotubes of 200nm in length could be obtained from Fe doped rutile powder, and have higher yields. The formation mechanism of long titania nanotubes was suggested in the light of the relative stability of crystalline phase.

【关键词】 水热法二氧化钛掺杂纳米管
【Key words】 hydrothermal method titania doping nanotube
【基金】 国家自然科学基金资助项目(No.20171039;50171036);浙江省自然科学基金资助项目(No.200053)
  • 【文献出处】 无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,2003年08期
  • 【分类号】O611.4
  • 【被引频次】108
  • 【下载频次】1286
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