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分光光度法测定雄黄及牛黄解毒片中可溶性砷的含量——牛黄解毒片中雄黄的系统研究(Ⅰ)
To Determine the Content of As in Niuhuangjiedu Tablet by Spectrophotometry The Systematic Study on Xionghuang in Niuhuangjiedu Tablet (Ⅰ)
【摘要】 目的 :对雄黄、牛黄解毒片中可溶性砷含量进行测定和比较。方法 :采用分光光度法。结果 :在 4~ 2 0μg范围内 ,线性关系良好 ( r=0 .9993) ;回收率为 99.1%。结论 :该方法灵敏度高 ,重现性好 ,可为牛黄解毒片含砷量限度制定提供依据
【Abstract】 Objective:To determine the soluble As in Niuhuangjiedu tablet and Xionghuang.Methods:The content of As is determined by spectrophotometry.Results:The linear range is 4~20 μg( r =0.999 3), the average recovery rate is 99.1 %.Conclusion:The method is sensitive and has good reproducibility.It can be used as a reference to the content limits of As in Niuhuangjiedu tablet.
【关键词】 分光光度法;
三氧化二砷;
牛黄解毒片;
雄黄;
【Key words】 Spectrophotometry; As 2O 3; Niuhuangjiedu tablet; Xionghuang;
【Key words】 Spectrophotometry; As 2O 3; Niuhuangjiedu tablet; Xionghuang;
【基金】 四川省教委自然科学基金资助项目 (No.1 999- 0 4 )
- 【文献出处】 时珍国医国药 ,LiShiZhen Medicine and Materia Medica Research , 编辑部邮箱 ,2003年04期
- 【分类号】R286
- 【被引频次】23
- 【下载频次】554