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CaO脱酸合成二辛基二甲基季铵盐

Synthesis of Dioctyl Dimethyl Quaternary Ammonium Salt in Removing Acid with CaO

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【作者】 黄展梁红冬

【Author】 HUANG Zhan,LIANG Hong-dong(Maoming College, Maoming, 52500 China)

【机构】 茂名学院化工学院茂名学院化工学院 广东茂名525000广东茂名525000

【摘要】 以二辛胺为原料,硫酸二甲酯为烷基化试剂,CaO为缚酸剂,通过非均相的液—固反应,常压下合成了二辛基二甲基氢氧化铵,二辛胺能定量转化。将二辛基二甲基氢氧化铵与盐酸或氢溴酸中和得到二辛基二甲基季铵盐。此方法反应时间短,反应产率高,一般可达98.2%,所得产品纯度高。

【Abstract】 Dioctyl dimethylammonium hydroxide is synthesized with dioctylamine as raw material, dimethyl sulfate as alkylating agent and calcium oxide as removing acid agent. The conversion of the dioctylamine is 100%.Diocty dimethyl quaternary ammonium salt is formed by using HC1 or HBr to neutralize diocty Dimethyl ammonium hydroxide. This reaction time is short, the reaction product prodult rate is high, which is general 98.2% ,and product is quite pure.

  • 【文献出处】 茂名学院学报 ,Journal of Guandong College Petrochemical Technology , 编辑部邮箱 ,2003年03期
  • 【分类号】TQ455
  • 【下载频次】70
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