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同质异形体SiC晶须与SiC颗粒的分离
Study on the separation of the paramorphic SiC whisker and SiC particle
【摘要】 在催化作用下利用稻壳为原料合成SiC晶须(SiCw)不可避免地产生同质异形体SiC颗粒(SiCp).烧成料通过筛分使SiCw富集于-100目的物料中,采用反浮选使富碳的SiCp得到去除,获得纯度为85%的SiCw初产品,调整矿浆的pH值至5 2,利用SiCw与SiCp的表面性质差异,采用浮选工艺成功地将微米级的SiCw与SiCp分离出来,获得纯度大于95%的SiCw,SiCw综合回收率达到83 76%.副产品β-SiCp增强SiC基质复合材料的热压制品磨耗比为标准砂轮的49 5倍.
【Abstract】 The paramorphic SiC particle (SiCp) was produced in the process of catalytic synthesis of SiC whiskers (SiCw) from rice hulls SiCw can be enriched in the sintered material minus 100 mesh by screening, then SiCw with purity of 85% was obtained after removing the carbonenriched SiCp by reverse flotation The micronmetergrade of SiCw and SiCp was satisfactorily separated by direct flotation based on the their surface difference in the condition of pH= 52 Consequently SiCw with purity over 95% was prepared The total recovery of the SiCw is 8376% The abrasion ratio of the hotpressed product of SiC matrix composite material reinforced with the β-SiCp is 495 times of that of the standard abrasive wheel
【Key words】 paramorph; SiC whisker; SiC particle; flotation; separation;
- 【文献出处】 煤炭学报 ,Journal of China Coal Society , 编辑部邮箱 ,2003年03期
- 【分类号】TQ163.4
- 【被引频次】5
- 【下载频次】153