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反相离子对高效液相色谱法测定溴氨酸
The Determination of Bromamine Acid with RPIP-HPLC
【摘要】 建立了一种测定溴氨酸的反相离子对 高效液相色谱的方法。以甲醇 水为流动相,四甲基溴化铵为离子对试剂,2 萘酚为内标物,检测波长为240nm,线性范围为0~0 18mg/ml,浓度测定的变异系数为0 26%~0 81%。
【Abstract】 The analysis method of bromamine acid was studied with RPIP HPLC. Chromatographic conditions are with methanol water was mobile phase, tetramethylammonium bromide as ion pair reagent, 2 naphthol as internal standard, and UV detection at 240nm. The method gives a linear range of O~0.18mg/mL and a coefficient of variation of 0.26%~0.81%.
【基金】 天津市自然科学基金项目(No.023606811);天津市教委科技发展基金项目资助课题(No.01-20510)
- 【文献出处】 精细化工中间体 ,Fine Chemical Intermediates , 编辑部邮箱 ,2003年04期
- 【分类号】O657.72
- 【被引频次】1
- 【下载频次】86