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X光透镜在X射线衍射技术中的应用

Applications of X-ray lens in X-ray diffraction techniques

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【作者】 王大椿陈俊李玉德赫业军颜一鸣

【Author】 WANG Dachun CHEN Jun LI Yude HE Yejun YAN Yiming ( Key Laboratory for Beam Technology and Materials Modification of Ministry of Education, Institute of Low Energy Nuclear Physics, Beijing Normal University, Beijing 100875 )

【机构】 北京师范大学射线束技术与材料改性教育部重点实验室北京师范大学低能核物理所北京师范大学低能核物理所 北京100875北京100875北京100875

【摘要】 用整体平行束X光透镜代替常规衍射仪的索拉狭缝和/或附加狭缝,入射和衍射X光强度可提高1.5―3.5倍,分辨率可达0.4°,可用于薄膜、粉末样品和离子束沉积样品的分析。将微会聚X光透镜应用于生物大分子衍射、高压X射线衍射、四圆X射线衍射3个不同的衍射领域,在相同X光源功率条件下,使用X光透镜后的衍射强度提高到原来的3―10倍,信噪比和分辨率有不同程度的改善。

【Abstract】 By using monolithic parallel beam X-ray lens instead of the attachment slits or Soller slits, the X-ray intensities both incident on and diffracted from the sample can be 1.5—3.5 times than the original and a resolution of 0.4°can be reached, thus the diffractional setup with X-ray lenses can be used to analyse thin film, powder and ion beam deposit samples. By using the slightly focusing X-ray lens in the macromolecular crystallography, high pressure and four circle X-ray diffractometers and at the same electric power supply, the diffracted intensities can be raised 3—10 times than the traditional diffractional equipment. In addition the signal to noise ratio and the resolution can be improved to a certain extent.

【关键词】 X衍射X光透镜平行束
【Key words】 X-ray diffractionX-ray lensParallel beam
  • 【分类号】O434.19
  • 【被引频次】3
  • 【下载频次】206
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