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预处理时间和温度对Al2O3p-TiCp/Al复合材料的反应温度特征的影响

Effect of pretreatment time-period and temperature on reactive temperature characteristics and microstructure of composite Al2O3p-TiCp/Al

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【作者】 寇生中许广济丁雨田丁宗富兰晔峰

【Author】 KOU Shengzhong, XU Guangji, DING Yutian, DING Zongfu, LAN Yefeng (College of Materials Science and Engineering, Gansu Univ. of Tech., Lanzhou730050, China)

【机构】 甘肃工业大学材料科学与工程学院甘肃工业大学材料科学与工程学院 甘肃兰州 730050甘肃兰州 730050甘肃兰州 730050

【摘要】 研究了预处理温度和时间对Al TiO2 C体系XD反应温度特征和复合材料组织的影响,结果表明,为了获得理想的Al2O3p TiCp/Al复合材料,预处理温度和时间有一个最佳的工艺范围.体系在本实验的工艺条件下,当预处理温度高于670℃时,由于反应程度加强,不利于体系在随后升温烧结过程中发生快速的放热反应,从而导致体系反应不完全.预处理时间小于30min,会导致体系反应不完全;预处理时间大于60min时,组织中Al3Ti含量增高.合适的预处理时间为30~60min,预处理温度为670℃.

【Abstract】 The effect of pretreatment temperature and timeperiod on characteristics of XD reaction temperature and microstructure of composite Al2O3pTiCp/Al in system of AlTiO2C is investigated. Result shows that there is an optimal region of pretreatment temperature and timeperiod for obtaining excellent composites Al2O3pTiCp/Al. In the present system and experimental condition, when the pretreatment timeperiod is less than 30 minutes, the reaction cannot take place completely. Otherwise, the composite would contain a lot of Al3Ti phases if pretreatment timeperiod were longer than 60 minutes. When the pretreatment temperature is above 670 ℃, too much reaction will take place during pretreatment, so that it is not favorable for subsequent XD reaction and makes the reaction incomplete. Optimal pretreatment timeperiod is 3060 minutes at temperature 670 ℃.

【基金】 甘肃省自然科学基金(ZS991 A25 051 C)
  • 【文献出处】 甘肃工业大学学报 ,Journal of Gansu University of Technology , 编辑部邮箱 ,2003年02期
  • 【分类号】TB331
  • 【下载频次】36
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