【Abstract】 Ternary metals disulfide nano-compound, Mn x(MoW) 1-xS 2, was prepared by exfoliating-restacking-structure controlling approach, and characterized by XRD, TEM, SAED and EDS respectively. XRD results show that the phases of the intermediate were composed of MoS 2, WS 2, MnCl 2·H 2O and one unclear phase. The end product was composed of MnS 2, MoS 2 and WS 2 phases. TEM results show that the morphologies of the sample are nano-tubular with ringent. EDS results show that the components of nanotube is Mn x(MoW) 1-xS 2. More detailed work is needed to study the precise structure and formation mechanism for sure.更多还原