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纯丝素凝胶的制备、结构和性能研究
Study of the Preparation and Structure and Properties of Pure Silk Fibroin Gel
【摘要】 利用双扩散原理,制备了纯丝素凝胶,并对其进行验证。结果表明纯丝素凝胶是一种具有多孔结构的淡黄色海绵状固体,结构中包含了无规卷曲、丝素Ⅰ、丝素Ⅱ三种不同的构象,并在低温(-4℃)结晶时,凝胶更易形成丝素Ⅰ构象。凝胶的断裂强度依赖于含水量。
【Abstract】 Pure silk fibroin gel (P5FG) was successfully prepared by the authors according to the bidifussion principles. The FSFC was verified by SME, IR and X-ray diffraction methods. The results showed that the PESG was a light - yellow spongy porous solid consisting of three kinds of conformations of random - coil, silk Ⅰ and silk Ⅱ, and the conformation of PSFG was easily converted to a - form during the crystallization at a lower temperature of - 4℃.
- 【文献出处】 纺织学报 ,Journal of Textile Research , 编辑部邮箱 ,2003年02期
- 【分类号】TS102
- 【被引频次】7
- 【下载频次】312