节点文献
乳化萃取技术抽提大豆磷脂中的磷脂酰胆碱
The Fractionation of Soya Lecithin with High Phosphatidylcholine Content Using Emulsification Extraction
【摘要】 利用乳化萃取设备 ,乙醇为溶剂 ,进行固液抽提于大豆磷脂中制备磷脂酰胆碱。通过正交实验得出优化的分离条件为 :抽提时间 10min ;抽提温度 - 10℃ ;磷脂 乙醇比 2 5g 30 0mL ;乙醇浓度 95 %。HPLC分析结果表明 :抽提后产品中磷脂酰胆碱的含量可以从原料中的 18.9%提高到 6 9.6 %。
【Abstract】 A new separation process was developed for the fractionation of soya lecithin with high phosphatidylcholine (PC) content using emulsification extraction. Granule lecithin was used as raw material and ethanol was used as the solvent. The optimal condition was established by orthogonal design. The extraction time is 10 min; extraction temperature is -10℃; phospholipids/solvent is 25 g in 300 mL; the concentration of ethanol is 95%. Under the optimal conditions, the PC content of soya lecithin was increased from 18.9% to 69.6%.
【关键词】 乳化萃取;
固液抽提;
大豆磷脂;
磷脂酰胆碱;
【Key words】 Emulsification extraction; solid-liquid extraction; soya lecithin; phosphatidylcholine;
【Key words】 Emulsification extraction; solid-liquid extraction; soya lecithin; phosphatidylcholine;
【基金】 黑龙江省自然科学基金资助课题 (B98- 2 2 )
- 【文献出处】 分析化学 ,Chinese Journal of Analytical Chemistry , 编辑部邮箱 ,2003年07期
- 【分类号】O658.2
- 【被引频次】11
- 【下载频次】264