节点文献
肉苁蓉挥发性化学成分分析
Analysis of Volatile Components in Herba Cistanches
【摘要】 报道了用同时蒸馏-萃取法提取肉苁蓉挥发性物质,测得肉苁蓉挥发油的含量为3.5%;利用GC/MS法分离确认出24种化学成分;用峰面积归一化法得出各化学成分在挥发油中的相对百分含量,其中主要成分为丁香酚,占总挥发油的83.60%;又用单离子法分离出丁香酚,并用IR,EI-MS法对其进行分析确认。
【Abstract】 The volatile components of Herba Cistanches were extracted by simultaneous distillation-extraction method and analyzed by combined capillary gas chromatography/mass speetrometry. Among 24 identified compounds the eugenol was mainly component. The relative content of eugenol was 83.60% in the all volatile components detected. The eugenol was isolated by single-ion method and identified by infrared spectrscopy and mass spectrometry.
【关键词】 肉苁蓉;
挥发性成分;
同时蒸馏-萃取;
丁香酚;
【Key words】 Herba Cistanches; volatile components; simultaneous distillation-extraction; eugenol;
【Key words】 Herba Cistanches; volatile components; simultaneous distillation-extraction; eugenol;
【基金】 辽宁省教育厅科学技术基金资助课题(No.20331079)
- 【文献出处】 分析化学 ,Chinese Journal of Analytical Chemistry , 编辑部邮箱 ,2003年05期
- 【分类号】O657.63
- 【被引频次】36
- 【下载频次】598