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比色管色谱法测定食品中甜蜜素的探讨

A Probe into Determination of Saccharin in Food by Gag Chromatography in Colorimetric Sylinder

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【作者】 侯晓燕李永芳李俊玲

【Author】 HOU Xiaoyan, LI Yongfang, LI Junling(Anyang Sanitation and Antiepidemic Station,Anyang 455000,China)

【机构】 安阳市卫生防疫站安阳市卫生防疫站 河南安阳455000河南安阳455000河南安阳455000

【摘要】 采用比色管为顶空瓶,顶空气相色谱法测定食品中甜蜜素含量。样品在比色管中保温,用氢火焰离子化检测器检测,食品中甜蜜素的最低检出浓度为1.9mg/kg,在样品中加标浓度为0.2-0.4g/kg时,平均回收率为92.4%-97.6%,高、中、低三种浓度的变异系数均小于5%。

【Abstract】 In this article, a colorimetric sylinder serves as a top-empty bottle, in which the sample is preserved in constant temperature , and the saccharin content in the food is determined by the gas chromatogram. The sample is tested by a hydrogen-fired ionometer. The tested minimus density of saccharin is 1.9mg/kg. When the density is increased to 0.2-0.4g/kg, the average rate of recovery is 92.4-97.6%, and the variation coefficent is under 5%, despite high, medium or low density.

  • 【文献出处】 安阳师范学院学报 ,Journal of Anyang Teachers College , 编辑部邮箱 ,2003年05期
  • 【分类号】TS207
  • 【被引频次】2
  • 【下载频次】53
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