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四根质谱直接进样分析重质油芳烃馏分烃类组成
Analysis of Aromatic Types in Heavy Distillates of Petroleum by Quadruple Mass Spectrometry with Direct Insertion Probe
【摘要】 本文介绍了用四极质谱直接进样测定重质馏份油芳烃烃类组成的方法,分析了仪器条件对实验结果的影响。实验操作简便,数据重复性好,通过与石科院分析结果的比较及掺对实验说明该方法比较准确可靠。
【Abstract】 The determinatlon of aromatic types in heavy distillates of petroleum by high ionizing voltage quadruple mass spectrometry with dlrect sample probe is described. The aromatic fraction is separated from heavy distillates of petroleum by sllica gel percolation and introduced directly into the EI ion source of the mass spectrometer by a direct insertion probe with a temperature programmed system. The influence of some conditions of mass spectrometer such as resolution, voltage and sample injection amount is discussed. The results show that veracity can be reflectcd by the intensity of the special mass of FC43 (standard sample).
【Key words】 hydrocarhon types; analysis method; heavy oil; aromatic;
- 【文献出处】 质谱学报 ,JOURNAL OF CHINESE MASS SPECTROMETRY SOCIETY , 编辑部邮箱 ,1998年04期
- 【分类号】O657.6
- 【被引频次】11
- 【下载频次】179