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喷涂功率对真空等离子喷涂羟基磷灰石涂层的影响

Effect of Spray Power on Characteristics of Vacuum Plasma Sprayed Hydroxyapatite Coatings

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【作者】 常程康石建民胡仲寅黄静琪丁传贤

【Author】 CHANG Cheng-Kang; SHI Jian--Min ;HU Zhong-Yin; HUANG Jing-Qi; DING Chuan-Xian (Shanghai Institute of Ceramics, Chinese Academy of Sciences Shanghai 200050 China)

【机构】 中国科学院上海硅酸盐研究所!上海200050

【摘要】 本文采用真空等离子喷涂设备(VacuumPlasmaSprnySystem),在不偷呐涂功率下制备了羟基磷灰石涂层,研究了热喷涂功率对羟基磷灰石涂层材料学特征的影响.实验中,使用X射线衍射仪,测定了涂层的相组成.使用扫描电子电镜,观察了羟基磷灰石涂层的表面形貌.研究结果表明,热喷涂功率对羟基磷灰石涂层的结构有着重大的影响.一方面,随着热喷涂功率的提高,涂层的非晶化加剧,涂层中非晶态的羟基磷灰石含量不断增大.另一方面,随着热喷涂功率的提高,羟基磷灰石粉末的熔化状态变好,颗粒之间的结合能力加强;涂层的显微结构明显改善.

【Abstract】 Hydroxyapatite coatings were made under different spray power using a Vacuum Plasma Spray System. The effects of spray power on characteristics of hydroxyapatite coatings were investigated.In the experiment, X Ray Diffeactometer and Scanning Electron Microscopy were used to detect phase compositions and microstructures of as-received coatings. The results obtained indicated that, plasma spray power greatly effected the characteristics of the as-received coatings. With the increase of spray power, hydroxyapatite content of as-received coatings decreased, showing the amorphorization of coatings was prompted. Also, with the increase of spray power, the melt of hydroxyapatite was improved, the coatings with good microstructures were obtained.

  • 【文献出处】 无机材料学报 ,JOURNAL OF INORGANIC MATERIALS , 编辑部邮箱 ,1998年02期
  • 【分类号】R318.08
  • 【被引频次】18
  • 【下载频次】229
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