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双烯合成反应与气相色谱法联合测定油品中共轭二烯烃含量的研究 Ⅱ.短毛细管柱气相色谱法
Study on the Method for Determination of Content of Conjugated Dienes in Petroleum Products by the Combination of Diene Synthesis Reaction with Gas Chromatography Ⅱ Short Capillary Column Gas Chromatography
【摘要】 在填充柱气相色谱法的基础上,使用12m×0.22mmi.d.的SE-30短毛细管柱(WCOT),分析了乙烯生产副产物——未加氢裂解汽油(55℃~220℃馏分)中共轭二烯烃的含量,分析一次需22min,内标物正十六烷得到了很好的分离。
【Abstract】 This paper is based on the packed column gas chromatography. By using a short capillary column (12m×0.22mmi.d.) coated with SE 30,the content of conjugated dienes in cracked gasoline (by product of ethene production without hydrogenation, with a boiling range of 55 220℃) could be determined. The analysis time of chromatography was 22min. A satisfactory separation of internal standard n Co16 with other components was obtained.
【关键词】 毛细管气相色谱法;
共轭双烯;
石油产品分析;
【Key words】 capillary gas chromatography; conjugated diene; petroleum product analysis;
【Key words】 capillary gas chromatography; conjugated diene; petroleum product analysis;
- 【文献出处】 色谱 ,CHINESE JOURNAL OF CHROMATOGRAPHY , 编辑部邮箱 ,1998年02期
- 【分类号】TQ53,O658
- 【被引频次】5
- 【下载频次】112