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SiC/W 纳米多层膜的微结构和微观力学性能
Microstructure and Micro Mechanics Analysis of SiC/W Nano Laminated Films
【摘要】 用磁控溅射法在硅基底上制备了不同调制波长Λ的SiC/W纳米多层膜,利用小角度衍射技术(LXD)研究了各样品子层界面的调制周期性,并用上限为20mN的超显微硬度计UMHT-3,对上述纳米薄膜进行了多载荷微观力学性能测试.结果表明:纳米SiC/W调制多层膜的超显微硬度随测试负荷F和调制波长Λ的改变而变化,在负荷为5mN时峰值硬度为19.9GPa,与均匀混合的纳米薄膜相比,超显微硬度值提高了约1倍,显示出明显的硬度异常效应.结合实验结果对硬度值随调制波长Λ出现的峰值效应作了初步探讨.
【Abstract】 SiC/W nano laminated films with various alternative lengths are prepared by a magnetron sputtering system. Using low angle X ray diffraction method, their interface miro structures and alternative periods are studied and the ultramicrohardness tests with loads smaller than 20 mN are performed on the nano laminated films by UMHT 3. It is shown that the UMH values of nano laminated films varies with the applied load F and alternative length Λ . When F =5 mN, the UMH reaches the maximum, 19.9 GPa, about one times higher than that of the homogeneously mixed layes. The anomalous UMH varying with the alternative length is discussed.
【Key words】 nano laminated film; microstructure; ultramicrohardness (UMH); alternative length;
- 【文献出处】 上海交通大学学报 ,JOURNAL OF SHANGHAI JIAOTONG UNIVERSITY , 编辑部邮箱 ,1998年02期
- 【分类号】O484.5
- 【被引频次】3
- 【下载频次】80