【摘要】 系统地研究了以Ｒａｎｅｙ镍为催化剂由葡萄糖和正辛胺形成Ｓｃｈｉｆ碱后催化加氢合成葡辛胺的反应，通过对反应条件的优化，特别是通过向反应体系中加入催化剂量的三乙胺，改善了催化剂的性能，降低了催化剂的用量，有效地抑制了副反应的发生，缩短了反应时间，反应产率达到７０％以上。并对失活的Ｒａｎｅｙ镍催化剂的再生进行了初步试探。更多还原

【Abstract】 nOctylDglucamine is prepared by catalytic hydrogenating the Schiff base formed from Dglucose and noctamine in the presence of Raney nickle. By adding Et3N, the side reactions are greatly restrained and the yield increases to 70%, the reaction time and the amount of Raney Ni are also reduced. The preliminary test is performed for the regeneration of the catalyst.更多还原