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高纯氧化镧中微量稀土杂质的化学光谱法测定

DETERMINATION OF TRACE RARE EARTH IMPURITIES IN THE HIGHPURITY LANTHANUM OXIDE BY CHEMICAL SPECTROGRAPHIC ANALYSIS

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【作者】 王淑英李武帅晏学晨彭春林

【Author】 WANG Shuying,LI Wushuai,YAN Xuechen and PENG ChunlinNational Analytical Research Center of Electrochemistry and Spectroscopy Changchun Institute of Applied Chemistry,Academia Sinica,130022 Changchun

【机构】 中国科学院长春应用化学研究所国家电化学和光谱研究分析中心

【摘要】 本文介绍了高纯氧化镧中微量稀土杂质的化学光谱测定,将La2O3通过P507萃淋树脂分离富集,将大量基体分离掉,剩下微量的稀土杂质,用C粉吸附后加KBH4做载体进行光谱测定。本方法可测定99.9999%纯度的La2O3中的微量稀土杂质。

【Abstract】 The determination of trace rare earth impurities in the highpurity Lanthanum oxide by chemical spectrographic analysis is reported in this paped.The matrix,La2O3,was separated by the extractioneluating resin P507.The remained rare earth impurities were absorpted by carbon powder.The rare earth impurities absorpted were determinated in carrier KBH4 by spectrographic analysis.The trace rare earth impurities in 999999% La2O3 can be determinated by this method.

  • 【文献出处】 光谱学与光谱分析 ,SPECTROSCOPY AND SPECTRAL ANALYSIS , 编辑部邮箱 ,1998年01期
  • 【分类号】O657.3
  • 【被引频次】5
  • 【下载频次】91
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