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用 234Th 为产额示踪剂、分光光度法测定环境水中钍的浓度
DETERMINATION OF THORIUM IN ENVIRONMENTAL WATERS USING 234 Th AS YIELD TRACER
【摘要】 本文介绍一种测定环境水中钍浓度的分析方法。10L环境水样用氢氧化铁沉淀法浓集钍,阴离子交换树脂除去杂质,分光光度法测定钍浓度。全过程用234Th作为产额示踪剂,进行回收率校正。方法探测下限为1.9×10-5Bq/L,回收率均值为(80.5±4.7)%。用本方法对本省11个地区的自来水、井水、河水、湖水及温泉水进行了分析,结果表明,各种水样中钍浓度的均值为0.20~2.63mBq/L。
【Abstract】 The paper introduces an analysis method of Th in environmental waters.The Th was concentrated by Fe(OH) 3 precipitation,separated from impurities by passing through a anion exchanger column,and determined by spectrophotometry. 234 Th was used as yield tracer.The average recovery was determined to be (80.5±4.7)%.The Th concentrations in water samples taken from 11 regions of Jiangsu province were determined,their average concentrations lie in the range of 0.20~2.63 mBq/L. (
【关键词】 钍;
浓度;
环境水;
分光光度法;
234Th;
产额示踪剂;
【Key words】 Thorium; Spectrophotometru; Concentration; Environmental Waters; 234 Th Yieid Tracer);
【Key words】 Thorium; Spectrophotometru; Concentration; Environmental Waters; 234 Th Yieid Tracer);
- 【文献出处】 辐射防护 ,RADIALIZATION PROTECTION , 编辑部邮箱 ,1998年03期
- 【分类号】TL271.4
- 【被引频次】4
- 【下载频次】97