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小角度晶界铜晶体的循环形变及饱和位错组态ECC观察

Cyclic Deformation Behavior and Observation of Saturation Dislocation Patterns of Copper Crystals Containing Low angle Grain Boundaries by SEM ECC Technique

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【作者】 张哲峰李小武苏会和陈道伦李广义王中光

【Author】 Zhang Zhefeng\ Li Xiaowu\ Su Huihe\ Chen Daolun\ Li Guangyi\ Wang Zhongguang (State Key Laboratory of Fatigue and Fracture for Materials, Institute of Metal Research, Academia Sinica, Shenyang 110015)

【机构】 中国科学院金属研究所材料疲劳与断裂国家重点实验室

【摘要】 通过对具有小角度晶界的铜晶体进行循环变形,发现其循环饱和切应力在塑性切应变范围0.6—4.7×10-3内基本不变(约为30MPa)。采用电子通道衬度(ECC)技术观察了其循环饱和时晶内、晶界及形变带附近的位错组态,发现在低应变幅下(γp1=0.6×10-3)晶内为驻留滑移带及脉络两相结构。随应变幅升高(γp1>1.7×10-3)驻留滑移带逐渐增多,最后形成规则的位错墙结构,并且位错墙连续穿过小角度晶界,在局部区域还发现小角度晶界两侧出现无位错区(DFZ);结合宏观形变带观察表明位错墙与形变带方向一致

【Abstract】 ? Cyclic deformation tests were carried out on copper crystal containg low angle grain boundaries under constant plastic shear strain amplitude control. It was found that the saturation resolved shear stress nearly maintains constant ( ̄30MPa) at the plastic resolved shear strain ranging from 0.6 to 4.7×10 -3 . Dislocation patterns within grains and in the vicinity of low angle grain boundaries were observed using electron channelling contrast (ECC) technique by SEM. The results show that the dislocation patterns consists of persistent slip bands (PSBs) and vein structures at the low plastic strain amplitude (γ p1 =0 6×10 -3 ). With increasing plastic strain amplitude, large volume fraction of persistent slip bands and regular dislocation walls were observed. Dislocation walls and persistent slip bands could cross through the low angle grain boundary continuously except that the dislocation free zones (DFZs) appeared at some local regions. Combining the observations of deformation bands, it was found that the dislocation walls are basically parallel to the deformation bands. 

【基金】 国家自然科学基金
  • 【文献出处】 电子显微学报 ,JOURNAL OF CHINESE ELECTRON MICROSCOPY SOCIETY , 编辑部邮箱 ,1998年03期
  • 【分类号】TN16,O763
  • 【被引频次】2
  • 【下载频次】235
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