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炎痛宁喷雾液中大黄素、盐酸小蘖碱的含量
Determination of Emodin and Berberine in Yantongning Spray
【摘要】 采用反相高效液相色谱法测定炎痛宁喷雾液中有效成分大黄素、盐酸小蘖碱的含量。结果大黄素在0.12~0.72μg范围内线性良好,r=0.9996,平均加样回收率为102.64%,RSD为1.56%;盐酸小蘖碱在0.022~0.154μg范围内线性良好,r=0.9993,平均加样回收率为99.86%,RSD为2.7%。
【Abstract】 WTBZ〗The determination of Emodin and Berberine in Yantongning Spray by HPLC was reported in this paper, A good linearity was shown at the concentration of 0.12 to 0.92 μ[WTBZ〗g of Emodin, r= 0.9996 , the average recovery rates is 102.64% and RSD is 1.06%. A good linearity was shown at the concentration of 0.022 to 0.154 μ[WTBZ〗g of Berberine, r= 0.9993, the average recovery rates is 99.86% and RSD is 2.7%. [WTHZ〗
【关键词】 炎痛宁喷雾液/化学;
大黄素/分析;
盐酸小蘖碱/分析;
HPLC;
【Key words】 WTBZ〗@ Yantongning Spray/chemistry; Emodin/analysis; Berberine/analysis; HPLC;
【Key words】 WTBZ〗@ Yantongning Spray/chemistry; Emodin/analysis; Berberine/analysis; HPLC;
【基金】 广东省自然科学基金
- 【文献出处】 中药新药与临床药理 ,TRADITIONAL CHINESE DRUG RESEARCH & CLINICAL PHARMACOLOGY , 编辑部邮箱 ,1997年03期
- 【分类号】R284.1
- 【被引频次】13
- 【下载频次】59