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Mo/α-Al2O3界面的二次离子质谱研究
SIMS Analysis of the Mo/α-Al2O3 Interface
【摘要】 采用电子束蒸发方法,在200℃的抛光(1102)取向的蓝宝石(α-Al2O3)单晶衬底上淀积厚度为300nm的Mo膜。经870℃下不同真空退火时间处理后,运用MCs+-SIMS技术进行了深度剖析,并结合XRD物相分析,对Mo/A2O3界面问题进行了探讨。结果表明,在Mo/Al2O3界面处存在原子相互扩散形成的过渡层。退火处理后,过渡层展宽,有MoO2生成。延长退火时间,过渡层变化不大。
【Abstract】 A 300 nm Mo film was deposited on a polished(1102) oriented sapphire substrate at 200℃by electron beam evaporation. Depth profiling was conducted using MCs+-SIMS technique after the samples were annealed at 870℃ for different time in high vacuum. Along with XRD analysis,the Mo/Al2O3 interfacial reaction was investigated. It was found that there was a transition layer formed due to the interdiffusion of atoms in the interface region. After annealing, the transition layer broadened, and a layer of MoO2 grew in the interface region,which hindered the inter-diffusion,so the transition layer changed a little with increasing the annealing time.
【Key words】 Mo/α-Al2O3 Interface; Secondary ion mass spectrometry; Depth profiling;
- 【文献出处】 真空科学与技术 , 编辑部邮箱 ,1997年04期
- 【分类号】TN301
- 【被引频次】1
- 【下载频次】40