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神乐片中钩藤碱的双波长薄层扫描定量法
Quantitative Determination of Rhynchophylline in Shenle Tablets
【摘要】 采用双波长薄层扫描法测定了神乐片中钩藤碱的含量。钩藤碱的最大吸收波长是253nm,参比波长是370nm。本法操作简便,结果较好,为控制产品质量提供了科学依据。
【Abstract】 The content of rhynochophylline in Shenle Tablets was examined by dualwavelength thin layer chromatography. The sample wavelength was 253 nm and the reference wavelength was 370 nm. Sx=3 and the slit was 1.2 nm×1.2 nm. This standard curve was linear within the range of 0 5 ̄5 μg and correlation coefficient was 0.9997. The average recovery was 98.40% ( n =5). This rapid, simple, sensitive and specific method is suitable for quality control of this product.
【关键词】 神乐片;
钩藤碱;
双波长薄层扫描法;
含量测定;
【Key words】 Shenle Tablets; Rhynchophylline; Dualwavelength thin layer chromatography scanning method; Determination of content;
【Key words】 Shenle Tablets; Rhynchophylline; Dualwavelength thin layer chromatography scanning method; Determination of content;
- 【文献出处】 中国药科大学学报 ,JOURNAL OF CHINA PHARMACEUTICAL UNIVERSITY , 编辑部邮箱 ,1997年02期
- 【分类号】O657.7
- 【被引频次】6
- 【下载频次】66