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有载体90Y-EDTMP的纸色层分离

STUDY OF 90 Y EDTMP PAPER CHROMATOGRAPHIC SEPARATION

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【作者】 白宏升金小海樊红强杜进刘跃民王凡陈大明许海林

【Author】 Bai Hongsheng Jin Xiaohai Fan Hongqiang Du Jin Liu Yuemin Wang Fan Chen Daming Xu Hailin (China Institute of Atomic Energy, Beijing 102413)

【机构】 中国原子能科学研究院同位素研究所

【摘要】 研究了有载体90Y-EDTMP在不同溶剂体系中的Rf和展开时间,以及浓氨水、乙醇和水体系溶剂配比和pH值对90Y纸色层分离的影响,同时与柱色谱、HPLC谱进行放射化学纯度比较。最后确定V(浓氨水)∶V(乙醇)∶V(水)=0.2∶2∶4,pH=9.0-14.0时分离效果最好

【Abstract】 The R f and the developing time of 90 Y EDTMP in different solvent system are studied. The effects of pH and solvent ratios on paper chromatographic behavior of 90 Y EDTMP are investigated in the ammonium hydroxide, ethanol and water system in detail.At the same time the results obtained here on the rediochemical purity of 90 Y EDTMP are compared with those of column chromatography and HPLC. It is found that when the solvent system of ammonium hydroxide, ethanol and water is used with the pH value fixed at 7.0-14.0, the best result would be obtained.

  • 【分类号】O658.1
  • 【下载频次】10
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