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鳙鱼心中电子载体泛醌化合物的研究
Study on Ubiquinone Compounds for Electron Carriers in Fish Heart
【摘要】 鳙鱼(Aristichthysnobilis)心脏提取物经硅胶柱色谱分离、制备薄层色谱纯化,得到二种泛醌化合物,用NMR、IR、MS、UV、HPLC、TLC等现代测试技术测定其化学结构为2,3-二甲氧基-5-甲基-6-10聚异戊二烯基-1,4-苯醌(Ⅰ)和一种未见报道的新泛醌酯——2,3-二甲氧基-5-甲基-6-甲酯基-八聚异戊二烯基-1,4-苯醌(Ⅱ)。
【Abstract】 Two ubiquinones were separated from heart extract of Aristichthys nobilis by silica gel column chromatography and purified by TLC.Their chemical structures were elucidated to be∶2,3 dimethoxy 5 methyl 6 (isoamylene) 10 1,4 quinone(Ⅰ)and a new ubiquinone ester,2,3 dimethoxy 5 methyl 6 methyl ester (isoamylene) 8 1,4 quinone(Ⅱ),by advanced instrumental analysis including NMR, IR, UV, MS, HPLC, TLC and chemical reactions.
【基金】 国家自然科学基金
- 【文献出处】 分析测试学报 ,JOURNAL OF INSTRUMENTAL ANALYSIS , 编辑部邮箱 ,1997年02期
- 【分类号】O656
- 【被引频次】1
- 【下载频次】34