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新植物生长调节剂“79401”在小麦及土壤中残留分析方法研究

A STUDY ON RESIDUE ANALYSIS METHOD OF NEW PLANT GROWTH REGULATOR “79401”IN WHEAT AND SOIL

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【作者】 冯秀琼; 高如瑜; 李琥; 赵秋霞;

【Author】 Feng Xiuqlong, Gao Ruyu, Li Hu, Zhao Qiuxia(The Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300071 )

【机构】 南开大学元素有机化学研究所!天津; 300071;

【摘要】 小麦及土壤中的植物生长调节剂“79401”用类似层析的方式,以甲醇-氨水混合溶剂洗提.洗提液通过调节不同PH值进行液-液分配得以净化.“79401”的两个主要组分01及02分别用萤光光度法和毛细管气相色谱法测定.方法平均回收率为84.5%~98.6%.变异系数为0.86%~16.09%.本残留分析方法已应用于田间试验样品的测定.

【Abstract】 The plant growth regulator "79401" was extracted with a mixed solvent of methanol-ammonia solution through a analogous to chromatographic mode. The extract was purifiedby liquid-liquid partition which was made in different pH value solution. The major twoingredient, 01 and 02, were determined by spectrofluorometry and capillary gas chro-matography respectively. The average recoveries of fortified 01 and 02 ranged from 84. 5%~98. 6% with coefficients of variation of O. 86% ~16. 09%. The method has been appliedfor the determination of the samples treated with "79401" in field trial

【关键词】 “79401”; 残留分析; 小麦; 土壤;
【Key words】 “794O1”; residue analysis; wheat; soil;
【基金】 国家自然科学专项基金
  • 【文献出处】 南开大学学报(自然科学版) ,JOURNAL OF NANKAI UNIVERSITY , 编辑部邮箱 ,1997年03期
  • 【分类号】S482.8
  • 【下载频次】46
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