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制取高纯试剂的一种新工艺

Study on New Process of the Preparation of High Purity Reagents

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【作者】 张广平

【Author】 Zhang Guangping

【机构】 武汉化工学院化工系

【摘要】 本文讨论了制取电容级的癸二酸、对硝基苯甲酸、苯甲酸、月桂酸及其铵盐等的新工艺。其工艺条件为:在有机酸中加入1~3倍高纯水通氨至pH为8左右,溶液脱色过滤后冷却结晶析出有机酸的铵盐,再将此铵盐加适量水溶解后用高纯度甲酸酸化。

【Abstract】 In this paper, a new process of preparing capacitor purity sebacic acid, p nitrobenzoic acid, benzoic acid, lauric acid, and their ammonium salts was discussed. The process conditions are that 1~3 times of high pure water was added to the organic acids and the ammonia pH about 8. The ammonium salts of the organic acids were crystalijed out from the solution after it was decolorized and filtered. Then the salts were dissolved into proper amount of high pure water, and the solution formed was acidified by high purity formic acid.

【关键词】 电容级试剂氨化有机酸
【Key words】 capacitor purity reagentammonifingorganic acids
  • 【文献出处】 辽宁化工 ,LIAONING CHEMICAL INDUSTRY , 编辑部邮箱 ,1997年02期
  • 【分类号】TQ420.6
  • 【被引频次】7
  • 【下载频次】90
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