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Preparation of γ-Al2O3 composite membrane and examination of membrane defects

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【作者】 李安武宏宾谷景华熊国兴

【Author】 LI Anwu ZHAO Hongbin GU Jinghuaand XIONG Guoxing(State Key Laboratroy of Catalysis,Dalian Institute of Chemical Physics,Chinese Academy of Sciences,Dalian 116023,China)

【机构】 State Key Laboratroy of CatalysisDalian Institute of Chemical PhysicsChinese Academy of SciencesDalian 116023ChinaChina

【摘要】 <正> A boehmite sol with a narrow particle size distribution and most probable diameter of 35 nm was prepared by peptization of boehmite suspension with HNO3 An unsupported γ-Al2O3 membrane made from the above sol possessed a narrow pore size distribution,with an average pore size of 4.8 nm and 320 m2/g specific surface area.A supported y-Al2O3 membrane produced by repeating dipping-drying-calcination procedure twice was proven to be defect-free by gas permeation measurements and SEM.

【Abstract】 A boehmite sol with a narrow particle size distribution and most probable diameter of 35 nm was prepared by peptization of boehmite suspension with HNO3 An unsupported γ-Al2O3 membrane made from the above sol possessed a narrow pore size distribution,with an average pore size of 4.8 nm and 320 m2/g specific surface area.A supported y-Al2O3 membrane produced by repeating dipping-drying-calcination procedure twice was proven to be defect-free by gas permeation measurements and SEM.

【基金】 supported by the National Natural Science Foundation of China
  • 【文献出处】 Science in China(Series B) ,中国科学B辑(英文版) , 编辑部邮箱 ,1997年01期
  • 【分类号】O614
  • 【被引频次】1
  • 【下载频次】38
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