【摘要】 采用１叔丁基３，３二硝基氮杂环丁烷为原料，通过苄氧羰基置换叔丁基，通氯化氢脱去苄氧羰基，合成了３，３二硝基氮杂环丁烷（ＤＮＡＺ）。将ＤＮＡＺ与ＮＴＯ、硝酸、高氯酸和硝仿反应合成了四种复盐，其中ＤＮＡＺ·ＨＣｌＯ４与ＤＮＡＺ·ＨＣｌ（ＮＯ２）３未见文献报道，经元素分析、红外、核磁共振光谱鉴定了化合物结构更多还原

【Abstract】 dinitroazetidine was prepared by treatment of 1 t(butyl) 3,3 dinitroazetidine with benzyl chloroformate and removal of benzyloxy carbonyl from the obtained 1 (benzyloxy carbonyl) 3,3 dinitroazetidine with hydrochloride Four energetic salts of 3,3 dinitroazetidine were prepared by mixing the free base with NTO, HNO 3,HClO 4 and nitroform respectively更多还原