节点文献

镧化合物催化合成醋酸异戊酯

A Study on Derivative UV-Spectrophotometric Method of Benzyl Alcohol and Benzaldehyde in Benzyl Alcohol Injection

  • 推荐 CAJ下载
  • PDF下载
  • 不支持迅雷等下载工具,请取消加速工具后下载。

【作者】 程延祥; 张洪生; 岳保尧; 郑奎强; 李晓红;

【Author】 He Nanfeng, Cheng Yanxiang,Li Hua (College of Chemistry and Chemical Engineering,Henan University,Kaifeng,475001)

【机构】 河南大学化学系;

【摘要】 考察了含镧化合物(La2O3、LaCl3、La-Y型分子筛)对醋酸异戊酯合成的催化活性,实验结果表明:三者的活性顺序为La-Y型分子筛>LaCl3>La2O3.La-Y型分子筛具有稳定的重复催化活性.

【Abstract】 A method was proposed for determination of benzyl alcohol in benzyl alcohol injection by the fouth order derivative UV-spectrophotometry.Benzaldehyde did not interfere with the determination of benzyl alcohol,when the concentration of benzaldehyde was less than 16 0 μg/ml.The calibration curve is linear in the concentration range of 180~400 μg/ml,and the relative standard derivation is less than 0 5%.The recovery of standard addition is from 99% to 101%.

【关键词】 镧; 催化; 分子筛; 醋酸异戊酯;
【Key words】 derivative spectrophotometry; benzyl alcohol; benzaldehyde;
  • 【文献出处】 河南大学学报(自然科学版) ,JOURNAL OF HENAN UNIVERSITY (NATURAL SCIENCE) , 编辑部邮箱 ,1997年02期
  • 【分类号】O621
  • 【下载频次】43
节点文献中: 

本文链接的文献网络图示:

本文的引文网络