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季戊四醇双缩醛的合成与表征
Preparation of Diacetal of Pentaerythritol with Heteropoly Acid as Catalyst
【摘要】 本文报道了用12-钨磷酸作催化剂合成了6种季戊四醇双缩醛,其结构用元素分析、IR及1HNMR等进行了表征。
【Abstract】 Diacetals of pentaerythritol were prepared by condensation of aldehydes with pentaerythriol in benzene with 12 tungstophosphoric acid as catalyst. The conditions of preparation have been pointed. The products were characterized by 1H NMR, IR and elemental analysis. The catalyst can be recovered conveniently.
- 【文献出处】 合成化学 ,CHINESE JOURNAL OF SYNTHETIC CHEMISTRY , 编辑部邮箱 ,1997年02期
- 【分类号】TQ25
- 【被引频次】21
- 【下载频次】243