节点文献
N-(4-乙酰氨基)苯基-3-羟基-2-萘甲酰胺的合成研究
Study on the Synthesis of N-(4-Acetylamino)phenyl-3-hydroxy-2-naphthalenecarboxamide
【摘要】 以2,3-酸和对氨基乙酰苯胺为原料合成N-(4-乙酰氨基)苯基-3-羟基-2-萘甲酰胺,研究了二种合成方法对产品纯度的影响,实验证明了钠盐法优于酸式法,产品含量>98%,反应收率818%。
【Abstract】 N-(4-Acetylamino)phenyl-3-hydroxy-2-naphthalenecarboxamide was prepared by N-acylation of 4-aminoacetanilide with 2-hydroxy-3-naphthoic acid or its sodium salt.The reaction conditions were studied.The yield and purity of two methods were 80.8% and 95% (acid method),81.8% and >98% (sodium salt method).
- 【文献出处】 染料工业 ,DYESTUFF INDUSTRY , 编辑部邮箱 ,1997年06期
- 【分类号】TQ612
- 【下载频次】75