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电感耦合等离子体-原子发射光谱法测定镍矿中镁的研究

DETERMINATION OF MAGNESIUM IN NICKEL ORE BY INDUCTIVE COUPLING PLASMA-ATOMIC EMISSION SPECTROMETRY

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【作者】 徐立张坚镛

【Author】 XU Li, ZHANG Jianyong(Guangzhou Research Institute of Non-Ferrous Metals)(Manuscript received 29 August, 1996)

【机构】 广州有色金属研究院!广州510651广州有色金属研究院

【摘要】 研究了电感耦合等离子体-原子发射光谱法(ICP-AES)测定镍矿中的镁.通过样品处理、酸度确定、谱线及仪器参数选择等试验,使方法操作简便快捷、结果科定、准确度较高.当镍矿中镁的含量分别为2.09%,8.12%和12.16%时,测量相对标准偏差分别为3.30%,1.35%和0.76%.当镁的含量为1.00%~4.00%时,加料回收率为99.5%~100.5%.

【Abstract】 Determination of Mg in Ni ore by ICP-AES has been studied. After testson the sample treatment, acidity influence, selection of spectrum lines and instrumentparameters, etc., it is found that this method is simple and rapid in operation; results aresteady and accuracy is high. When the Mg contents in Ni ore are 2. 09%, 8.12% and12. 16%, respectively, the relative standard deviations in determination are 3. 30%, 1. 35%and 0. 76%, respectively. When the Mg contents lie between 1. 00%~4. 00%, the additionrecoveries are between 99. 5 % ~100. 5 %.

  • 【文献出处】 广东有色金属学报 ,JOURNAL OF GUANGDONG NON-FERROUS METALS , 编辑部邮箱 ,1997年01期
  • 【分类号】O657.3
  • 【被引频次】1
  • 【下载频次】66
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