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2-乙基己醇催化脱氢制备2-乙基己酸

2-Ethylhexanoic Acid Prepared by Catalytic Dehydrogenation of 2-Ethylhexanol

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【作者】 李专成

【Author】 Li Zhuanchen (Fujian Provincial Institute of Chemical Industrial Science and Technology,Fuzhou,350013)

【机构】 福建省化工研究所

【摘要】 采用2-乙基己醇常压催化脱氢制备2-乙基己酸.进行了工艺条件试验,确立了较佳的工艺条件,产品得率>87%,产品纯度≥99%.

【Abstract】 Ethylhexanoic acid is prepared by reacting 2-ethylhexanol with sodium hydroxide in the presence of alkali-earth metal catalyst and under atmosphere. The amount of the catalyst added has significant effect on the reaction rate and better technological conditions are established,which are as follows:molecular ratio of 2-ethylhexanol to sodium hydroxide:1.4∶1;temperature:210 ℃;reaction period:6H;under above conditions,the yield of product is over 87% and the purity is 99%.

  • 【文献出处】 福州大学学报(自然科学版) ,JOURNAL OF FUZHOU UNIVERSITY(NATURAL SCIENCES EDTION) , 编辑部邮箱 ,1997年03期
  • 【分类号】O623
  • 【被引频次】4
  • 【下载频次】171
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