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用激光激发原子荧光光谱仪测定南极冰雪样品中铅含量

Laser Excited Atomic Fluorescence Spectrometer and Lead Content Determination of Antarctic Ice-Snow Sample

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【作者】 薛猛陈瓞延文克玲李良权李晖衣嵘马万云张骏秦大河孙俊英李淑玲

【Author】 Xue Meng, Chen Dieyan. Wen Keling. Li Liangquan,Li Hui, Yi Rong, Ma Wanyun, Zhang Jun (Department of Modm Applied Physics, Tsinghua University, Beijing 100084) Qin Dahe, Sun Junying (Lanzhou Institute of Glaciology and Geocryology, Chinese Academy of Scie

【机构】 清华大学现代应用物理系!北京 100084清?

【摘要】 自行研制的原子荧光光谱仪,由无焰石墨炉原子化器、准分子激光器泵浦的脉冲染 料激光器等组成。用其对95个南极冰雪样品中的铅进行了测量,其含量在4×10-12~4.7× 10-11g/mL之间。本方法的检出限为0.2×10-12g/mL,精密度为7%。

【Abstract】 This paper reports a newly designed laser excited fluorescence spectrometer. It consists of a graphite furnace electrothermal atomizer and an excimerlaser pumped dye laser. This spectrometer has been applied to the analysis of 95 Antarctic ice-snow samples. Results show that the Pb content in samples ranges from 4 × 10-12 to 47 × l0-12 g/mL. A detection limit of 0. 2× 10-12 g/mL and a precision of 7% are obtained.

  • 【文献出处】 分析化学 ,Chinese Journal of Analytieal Chemistry , 编辑部邮箱 ,1997年05期
  • 【分类号】O657.3
  • 【被引频次】10
  • 【下载频次】100
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