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应用反应精馏法生产高纯度醋酸甲酯的实验研究Ⅱ.半连续反应精馏
Experimental Study on Production of High Purity Methyl Acetate via Reactive Distillation
【摘要】 以醋酸和甲醇为原料,应用半连续反应精馏法生产高纯度醋酸甲酯,并对影响产品纯度的几个主要参效及操作条件(包括催化剂浓度、醋酸和甲醇的摩尔比、进料速率、回流比)进行了探讨。
【Abstract】 This paper presents the experimental results of producing high purity methyl acetate via the reaction of methanol and acetate acid, by using the method of semi-continuous reactive distillation. The main factors and the suitable operating conditions: the catalyst concentration, HOAc/MeOH mole ratio、feed flow rate and reflux ratio, which affect the purity of product, are discussed in this paper.
【关键词】 半连续法;
反应精馏;
醋酸甲酯;
持液量;
填料塔;
【Key words】 Semi-continuous; Reactive distillation; Methyl acetate; Liquid hold-up; Packed column;
【Key words】 Semi-continuous; Reactive distillation; Methyl acetate; Liquid hold-up; Packed column;
- 【文献出处】 中国药科大学学报 ,Journal of China Pharmaceutical University , 编辑部邮箱 ,1996年10期
- 【分类号】TQ225.24
- 【被引频次】10
- 【下载频次】197