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纳米SnO2微粉的制备与性能
Preparation and Properties of Nanometer-Sized SnO2 Powder
【摘要】 纳米SnO2微粉的制备与性能刘杏芹,陶善文,沈瑜生(中国科学技术大学材料科学与工程系合肥230026)关键词纳米微粉,二氧化锡,溶胶-凝胶法,气敏性能SnO2作为一种功能基体材料,在气敏、湿敏、光学技术等方面已有广泛的应用,而SnO2微粉或超微粉的?..
【Abstract】 Ultra-fine SnO2 powder with mean size of 2~3 nm was prepared by a sol-gel process.The structure and properties of the powder were studied.It is found that the tetragonal tin dioxide formed essentially during the gel drying at 70℃,and further crystallized on heating at 240~330℃,which was much lower than the temperature reported for the powder prepared with other method.The temperature dependent curue of conductivity for the thick film gas sensors made of this ultrafine powders showed a peak at 130℃,which was obviously lower than that reported in literature.The gas sensing layer of the element exhibited good strength and good resistivity stability as well as high sensitivity to H2 and C2H2 gases.
【Key words】 nanometer-sized powder; SnO2; sol-gel process; gas sensing property;
- 【文献出处】 应用化学 ,CHINESE JOURNAL OF APPLIED CHEMISTRY , 编辑部邮箱 ,1996年01期
- 【分类号】TB383
- 【被引频次】65
- 【下载频次】455