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含异硫氰酸苯酯裂解碎片的铁硫羰合簇取代衍生物的合成与表征

SYNTHESESAND CHARACTERIZATION OF IRON CARBONYL CLUSTERS WITH PHENYLISOCYANIDO AND THIO LIGANDS FROM CLEAVING OF THE PHENYLISOTHIOCYANATE

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【Author】 L u Qingwei Wang Yibing Wu Baoshan Suo Quanling Liu L ianyun Zhi Jiwu (Departmentof Chemical Engineering,Inner Mongolia Polytechnic University,H uhehaote 0 1 0 0 62 ) Liu Shutang Hu Xiang (Departmentof Chemistry,Inner Mongolia University,H uhehaote 0 1 0 0 2 1 )

【机构】内蒙古工业大学化学工程系；内蒙古大学化学系；内蒙古大学化学系呼和浩特010062；呼和浩特010062；呼和浩特010021；呼和浩特010021；

【Abstract】 New mono- and di- substituted derivatives of Fe3 (CO) 9(μ3 - S) 2 were synthesized by reac- tion of C6H5NCS with Fe3 (CO) 1 2 atroom temperature.Their structure were characterized by means of IR(νCO) ,MS,1 H NMR,1 3 C NMR,elemental analysis and X- ray four cycle diffrac- tometer.The results showed that the formulas of the cluster compounds are Fe3 (CO) 8 (CNC6H5) (μ3 - S) 2 and Fe3 (CO) 7(CNC6H5) 2 (μ3 - S) 2 respectively.更多还原

【关键词】裂解碎片；三核铁簇；合成；
【Key words】 synthesis cleaving fragment trinuclear iron；

【基金】内蒙古自然科学基金;兰州化物所 OSSO开放室基金资助项目

【文献出处】无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,1996年01期

【分类号】O627.8
【下载频次】31

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