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系数倍率分光光度法测定安钠咖注射液的含量

K-RATIO SPECTROPHOTOMETRIC ASSAY OF ANNAKA INJECTION

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【作者】 陈晓辉张旭明任雪冬张敏

【Author】 Chen Xiaohui; Zhang Xumin; Ren Xuding(Liaoning Institute of Physical Testing and Chemical Analysis Shenyang 110015)Zhang Min(Shenyang the Sixth People’s Hospital, Shenyang 110006)

【机构】 辽宁省分析测试研究中心!沈阳110015沈阳市第六人民医院!沈阳110006

【摘要】 本文提出以系数倍率分光光度法测定安钠咖注射液中咖啡因和本甲酸钠的含量.样品以0.1mol/LHCl液稀释后,在230nm和272nm波长处同时测定咖啡因和本甲酸钠,测得二组分平均回收率分别为99.1%和100.2%,相对标准差为0.77%和0.76%(n=7).本法简便、快速,适用于安钠咖注射液的常规分析.

【Abstract】 A K-ratio spectrophotometric method for the quantitative determination of caffeine and sodium benzoate in annaka injection was investigated by using manual spectrophotometer (UV-300). The sample diluted with 0. 1 mol/L HCL solution, was analyzed by absorbances at 230 nm and 272 nm. The average recoveries were 99.1 % and 100. 2% respectivly and the coefficients of variation were 0.77% and 0. 76% (n=7). Linearity and precision of analysis are good and the method is easy to carry out.

  • 【文献出处】 沈阳药科大学学报 ,Journal of Shenyang Pharmaceutical University , 编辑部邮箱 ,1996年01期
  • 【分类号】R927.2
  • 【被引频次】2
  • 【下载频次】15
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