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氯甲酸三氯甲酯法合成DV-菊酰氯
Synthesis of DV-Chrysanthemyl Chloride from Trichloromethyl Chloroformate
【摘要】 本文报道了由DV-菊酸甲酯经皂化、酸化制得DV-菊酸,然后用氯甲酸三氯甲酯酰氯化合成DV-菊酰氯,含量达到94.5%,酰氯化收率达到96%。
【Abstract】 A new preparation method of DV-chrysanthemyl chloride was described in this paper.Methyl DV-chrysanthemate via saponification,acidification and then chlorination by trichloromethyl chloroformate to give DV-chrysanthemyl chloride.The purity of the product was 94.5%.and yield of chlorination was 96%.
- 【文献出处】 农药 ,PESTICIDES , 编辑部邮箱 ,1996年12期
- 【分类号】TQ453.292
- 【被引频次】1
- 【下载频次】177