节点文献
双黄隆反相高效液相色谱分析
Analysis of Shuanghuanglong by Reversedphase High performance Liquid Chromatography
【摘要】 本文报道用反相高效液相色谱分析双黄隆可湿性粉剂,其有效成分甲黄隆、绿黄隆含量的方法,以甲醇和1%乙酸钠水溶液作流动相,以香豆素为内标物,在254纳米下检测。甲黄隆、绿黄隆变异系数分别为0.34%、0.61%。
【Abstract】 In this paper.a reversed-phase high performance liquid chromatography method to determine two active ingredients of Shuanghuanglong consisting metsulfuron-methyl and chlorsulfuron was described.Chromatographic conditions were:clolumn, Nova-Pak C18,5μ,3.9mm×150mm; mobile phase,MeOH:H2O:NaAc (30:70: 0. 7, v/v/m); internal standard , coumarin;flow rate,1.2ml/min;deteded at 254nm.The variation coefficient were 0. 34%and 0. 61%, respectively.
【关键词】 双黄隆;
甲黄隆;
绿黄隆;
反相高效液相色谱;
【Key words】 Shuanghuanglong; metsulfuron-methyl; chlorsulfuron; reversed-phase high performance liquid chromatography.;
【Key words】 Shuanghuanglong; metsulfuron-methyl; chlorsulfuron; reversed-phase high performance liquid chromatography.;
- 【文献出处】 农药 ,PESTICIDES , 编辑部邮箱 ,1996年06期
- 【分类号】TQ457.207
- 【下载频次】27