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铁邻菲咯啉、8-羟基喹啉配合物/Y型分子筛的制备、表征及催化苯酚羟化的研究

Studies on Preparation of Iron Phenanthroline and 8 - Hydroxyquinoline Complexes/Y Zeolite, Characterization and Catalytic Hydroxylation of Phenol

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【Author】 Qi Xing - Yi Wang Guo-Jia(Department of Chemistry, Jilin University, Changchun, 130023)Yue Xing-Kai Wu Yue(Changchun Institute of Applied Chemistry, The Chinese Academy of Sciences , Changchun , 130022)

【机构】吉林大学化学系；中国科学院长春应用化学研究所；中国科学院长春应用化学研究所长春130023；长春130023；长春130022；长春130022；

【摘要】制备了铁邻菲咯啉、8-羟基喹啉配合物/Y型分子筛(简记为FePhen/Y,FeO_x/Y).用元素分析,TG-DTA,UV-Vis,IR,SEM,BET,及XRD等方法确定了分子筛笼中金属配合物的生成及其晶体结构,考察了实验参数对苯酚转化率及产物选择性的影响.更多还原

【Abstract】 Iron phenanthroline - and 8 - hydroxyquinoline complexes /Y zeolite, denoted as FePhen/Y and FeOx/Y respectively, were prepared; The formation of the metal complexes mentioned above within the cages of Y zeolite and their crystal structures were determined by elemental analyses, diffuse reflectance UV - Vis,SEM,BET,and XRD methods;The influence of experimental parameters upon phenol conversion and product selectivities were investigated as well.更多还原

【关键词】邻菲咯淋； 8-羟基喹啉；分子筛；苯酚羟化；

【基金】国家自然科学基金资助课题

【文献出处】化学学报 ,Acta Chimica Sinica , 编辑部邮箱 ,1996年10期

【分类号】O643.3
【被引频次】6
【下载频次】118

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