【摘要】 本文报道了电化学氧化法制备偶氮二甲酰胺的研究．在最佳条件下恒电流电解联二脲的悬浮体系制得偶氮二甲酰胺，产率９６％，电流效率９４％左右．产品质量符合中华人民共和国化工行业优等品标准．电解时阳极过程遵循ＥＣＥＣ机理．更多还原

【Abstract】 In this work,azobisformamide was prepared by electro-oxidation method.In optional condition,We prepared azobisformammide by oxidation electrolysising the suspended substance of biurea. The yiuld could reach above 96%,the current efficiency about 94%. The quality of azobisformamde accordes with the Chinese chemical industry standard of high quality product,The anode properties adhere to ECECmechanism.更多还原