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固载型杂多酸催化合成尼泊金丁酯
The Synthesis of Butylparasept by Solid Hetropolyacid Catalyst
【摘要】 本文用12-钨磷酸(HPW)作为对羟基苯甲酸与正丁醇酯化合成尼泊金丁酯的固体催化剂。研究了不同的载体及制备方法、醇酸配比对酯收率的影响。初步考查了催化剂的稳定性。回流吸附法制备的HPW/活性炭具有酯收率高、稳定性好、不易流失等优点。
【Abstract】 In this paper,12-tungstophosphoric acid is used as solid catalyst for the esterification d butanol and p-hydroxybenzoic acid.The effect of such factors as different carrier,different synthesis technology and the ratio of butanol to the acid, on the yield of the ester have been studied. The stability of catalyst have been investigated preliminarily.
【关键词】 12-钨磷杂多酸;
尼泊金丁酯;
接触催化;
【Key words】 tungstophosphoric acid(HPW); Butyl chemosept; Contact catalysis;
【Key words】 tungstophosphoric acid(HPW); Butyl chemosept; Contact catalysis;
- 【文献出处】 黑龙江大学(自然科学学报) ,JOURNAL OF NATURAL SCIENCE OF HEILONGJIANG UNIVERSITY , 编辑部邮箱 ,1996年03期
- 【分类号】O623.624.3
- 【被引频次】11
- 【下载频次】104