节点文献
高效毛细管电泳-电导分析仪的组装及其在碱金属离子及氨基酸分离与测定中的应用
Assembling of a High Performance Capillary Electrophoretic Apparatus With Conductometer Detector and Its Application to the Determination of Alkali Metal Ions and Amino Acids
【摘要】 本文叙述了制作微型电导池的一种方法。用微型电导池、直流高压发生器、电导仪、记录仪等组装了一套高效毛细管电泳-电导检测装置。HPCE-CD装置已被用于天然矿泉水中碱金属离子及人发中氨基酸的测定。获得的结果是令人满意的。在最佳实验条件下,对Li-Na-、K-的检测限分别为5.0×108mol/L。
【Abstract】 A method for making micro conductivity cell was described. An instrument ofHPCE and CD was assembled with a micro conductivity cell, direct current high voltage generator. conductometer, recorder etc. and used for the determination of alkali metal ions innatural mineral water and amino acids in human hair. Results obtained were satisfactory.The limit of detection is 5. 0 ×10 8mol/L for ions Li’, Na+ and K+ in optimum experimentalconditions .
【关键词】 高效毛细管电泳;
电导法;
碱金属离子;
氨基酸;
【Key words】 High Performance capillary electrophoresis; conductometry; alkali metal ion; amino acid;
【Key words】 High Performance capillary electrophoresis; conductometry; alkali metal ion; amino acid;
【基金】 国务院侨办重点学科科研基金
- 【文献出处】 分析化学 ,Chinese Journal of Analytieal Chemistry , 编辑部邮箱 ,1996年11期
- 【分类号】O657.1
- 【被引频次】6
- 【下载频次】163