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非晶态PdCuSi的内耗和DSC研究

A STUDY OF THE AMORPHOUS PdCuSi ALLOY BY INTERNAL FRICTION AND DSC MEASUREMENTS

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【作者】 水嘉鹏陈秀梅王灿

【Author】 SHUI Jiapeng; CHEN Xiumei;WANG Can (Laboratory of Internal Friction and Defects in Solid,Institute of Solid State Physics,Chinese Academy of Sciences)(Correspondent:SHUI Jiapeng,Institute of Solid State Physics,Chinese Academy of Sciences,Hefei 230031)

【机构】 中国科学院固体物理研究所内耗与固体缺陷开放研究实验室

【摘要】 用葛摆测量了a-PdCuSi合金的内耗-温度曲线,证明在该合金的Tg和Tx温度附近有两个内耗峰P1和P2.P2峰是与非晶晶化有关的内耗峰,而P1峰可能是弛豫型的内耗峰.分析了倒扭摆和Collette摆的灵敏度,阐述了这两种摆不适用于测量a—PdCuSi类合金的内耗峰.

【Abstract】 he internal friction of the amorphous Pd77.5 Cu6.0 Si16.5 alloy (a-PdCuSi) was measured with a conventional torsion Pendulum(Ke torsion pendulum)in ascending temperatres and it was evident that there were two internal friction Peaks (p1 and p2 peaks) near the glass transition temperature Tg and the crystallization temperature Tx of a-PdCuSi alloy respectively. From DSC measurement,it was found that the origin of P2 peak was directly related to the crystallization,while p1 peak may be a relaxing peak. The sensitivity of the inverted torsion pendulum and the Collette Pendulum were discussed. Authors have found that the measured results of internal friction on a-PdCuSi alloy with the inverted torsion pendulum or the Collette pendulum are unbelievable.

【关键词】 非晶态内耗峰DSC
【Key words】 amorphous alloy internal friction peak DSC
  • 【文献出处】 材料研究学报 ,CHINESE JOURNAL OF MATERIAL RESEARCH , 编辑部邮箱 ,1996年03期
  • 【分类号】TG139.8
  • 【下载频次】71
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