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含有β-二酮结构热致性液晶聚醚酮的合成
Thermotropic Liquid Crystalline Polyetherketone with β diketone Spacer
【摘要】 该文首先合成了新单体1,3-二(4′-羟基苯基)-1,3-丙二酮,然后与不同的1,n-二卤代烷缩合得到了一系列含有β-二酮结构的热致性液晶聚醚酮,并对之进行了初步分析和表征
【Abstract】 In this paper,we have firstly prepared a new monomer,1,3 bis(4’ hydroxylbenzyl) propane 1,3 diketone from ethyl p methoxylbenxyl ethyl ketone in high yield and high purity.And then,being empolyed it,three themotropic liquid crystalline polytherketone with β diketone spacer had been gotten by polycondensation with 1, n dihalogenoalkane( n =3,4,5) and characterized by elemental analysis,IR,DSC and polarized hot stage microscopy.
【基金】 江西省自然科学青年基金
- 【文献出处】 江西师范大学学报(自然科学版) ,JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION) , 编辑部邮箱 ,1996年03期
- 【分类号】O631
- 【被引频次】1
- 【下载频次】46