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血清中微量锌的示波极谱法测定

Determination of Trace Zinc in Serum by Oscilloscope Polarography

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【作者】 张洪权; 朱景阳; 吴予明; 常爱武; 朱汝瑾; 刘继康;

【Author】 Zhang Hongquan Zhu Jingyang Wu Yuming Chang Aiwu Henan Medical University(450052,Zhengzhou)Zhu Rujin Liu Jikang Zhengzhou University(450052,Zhengzhou)

【机构】 河南医科大学; 郑州大学; 郑州大学 郑州 450052; 郑州 450052; 郑州 450052;

【摘要】 本文提出了运用单扫描示波极谱测定血清中锌的方法。在NH4OH-NH4Cl底液中,锌离子在-1.39V(相对饱和甘汞电极)有一灵敏还原波,此波可在0.01~100μg/ml范围内检测锌。将该法用于血清锌含量的分析,结果满意。

【Abstract】 A sensitive and selective method is presented for the direct determination of trace zinc in serum by linear scaning polarog-raphy. In NH1OH-NH1Cl substrate solution. a sharp reductive peak relating to the concentration of zinc ion appears at -1-39v(VS. SCE). The peak height is proportional to the con-centration of zinc ion over a range of 0. 01μg/ml. Several samples of zinc in serum have been analyzed by the recommended procedure and the results agree well with the statistical analysis.

【关键词】 锌; 血清; 极谱;
【Key words】 Zinc Serum Cathodic stripping voltammetry;
  • 【文献出处】 中国卫生检验杂志 ,Chinese Journal of Health Laboratory Technology , 编辑部邮箱 ,1995年03期
  • 【分类号】R446.1
  • 【被引频次】1
  • 【下载频次】27
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