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电弧法制备富勒烯的条件
EXPLORATION OF SYNTHESIZING FULLERENES
【摘要】 研究了用电弧法生产富勒烯(fullerene)的条件。通过实验,分析了石墨棒的直径、电压、起弧电流和氦气压力对产率的影响。得到生产富勒烯的最佳条件:电压25~30V;氦气压力2.7×103~6.7×103Pa;电流100±10A(对66mm碳棒),150±10A(对68mm碳棒)和200±10A(对d10mm碳棒);产率与碳棒直径无关。
【Abstract】 The condition for the preparation offullerenes was studied using the graphite- plasmadischarge method.Four factors were considered : diameter of graphite rod, voltage,electriccurrent, and the pressure of helium. An effective condition was obtained as follows:voltage 25~30V pressure of He 2. 7×10 ̄3~6.7×10 ̄3pa current 100±10 A( for d 6 mm rod)150±10 A( for d 8 mm rod)200±10A(for d 10 mm rod)
【基金】 中国有色金属工业总公司高新技术和新材料科研基金
- 【文献出处】 中南工业大学学报 , 编辑部邮箱 ,1995年02期
- 【分类号】O613.71
- 【被引频次】7
- 【下载频次】151